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Beilstein J. Org. Chem. 2020, 16, 502–508, doi:10.3762/bjoc.16.45
Graphical Abstract
Scheme 1: Reaction modes of alkyne.
Figure 1: Substrate scope of 1 and 2. aConducted at 80 °C for 24 h in MeCN with CuBr (10 mol %), 1,10-Phen (2...
Scheme 2: Proposed mechanism.
Scheme 3: Control experiment.
Scheme 4: Reaction of 2a and 4a.
Figure 2: Substrate scope of 2 and 4. aConducted at 100 °C for 20 h in 1,4-dioxane with CuI (10 mol %), 1,10-...
Beilstein J. Org. Chem. 2013, 9, 1326–1332, doi:10.3762/bjoc.9.149
Figure 1: ORTEP structure of trans-2a.
Scheme 1: Formation of bicyclic dihydrosilole 2a under high concentration conditions.
Scheme 2: Plausible reaction mechanism.
Scheme 3: Reaction 1a with Et3GeH.